N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide

Base Information

• Chemical Name: N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide
• CAS No.: 1616666-60-4
• Molecular Formula: C₂₅H₂₉BrN₂O₂S
• Molecular Weight: 501.487

Synonyms:N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide

Chemical Property of N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide

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Technology Process of N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide

There total 1 articles about N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-((4-(tert-butyl)phenyl)sulfonyl)-2-phenylaziridine + 2-bromobenzylamine (3959-05-5) → N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide (1616666-60-4)

Guidance literature:

With lithium perchlorate; In acetonitrile; at 20 ℃; for 5h; regioselective reaction; Inert atmosphere;

DOI:10.1021/jo500888j

Reference yield: 81.0%

N-(2-((2-bromobenzyl)amino)-2-phenylethyl)-4-(tert-butyl)-benzenesulfonamide (1616666-60-4) → 5-((4-(tert-butyl)phenyl)sulfonyl)-7-phenyl-5,6,7,9-tetrahydro-4bH-dibenzo[c,e]imidazo[1,2-a]azepine

Guidance literature:

With copper(l) iodide; sodium hydride; L-proline; In N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;

DOI:10.1021/jo500888j

upstream raw materials:

2-bromobenzylamine

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