phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside
CAS No.:1262015-27-9
Molecular Formula:C₃₅H₃₀O₈S₂
Molecular Weight:642.75
Hs Code.:

Synonyms:phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

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Technology Process of phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

There total 1 articles about phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 945626-51-7
phenyl 2,3,6-tri-O-benzoyl-1-thio-β-D-galactopyranoside

: 358-23-6
trifluoromethylsulfonic anhydride

: 1262015-27-9
phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

Guidance literature:: phenyl 2,3,6-tri-O-benzoyl-1-thio-β-D-galactopyranoside; trifluoromethylsulfonic anhydride; With pyridine; In dichloromethane; at 0 ℃; for 1h; Under argon atmosphere;

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; potassium thioacetate; at 20 ℃; for 1.5h;
DOI:10.1016/j.carres.2010.10.001

Reference yield: 78.0%

: 1262015-27-9
phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside

: phenyl 1,4-dithio-β-D-glucopyranoside

Guidance literature:: phenyl 1-thio-4-S-acetyl-2,3,6-tri-O-benzoyl-4-thio-β-D-galactopyranoside; With sodium methylate; In methanol; at 20 ℃; for 48h; Under argon atmosphere;

With diothiothreitol; In water; at 20 ℃; Under argon atmosphere;
DOI:10.1016/j.carres.2010.10.001