3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

Base Information

Chemical Name:3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate
CAS No.:1416009-56-7
Molecular Formula:C₂₉H₂₅NO₆SSi
Molecular Weight:543.672
Hs Code.:

Synonyms:3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

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Chemical Property of 3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

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Technology Process of 3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

There total 3 articles about 3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 58851-99-3
3-benzothiazol-2-yl-7-hydroxy-chromen-2-one

: 207342-30-1
2-(trimethylsilyl)ethyl hydrogen phthalate

: 1416009-56-7
3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo301698v

Reference yield:

: 85-44-9
phthalic anhydride

: 1416009-56-7
3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo301698v

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 1416009-56-7
3-(benzo[d]thiazol-2-yl)-coumarin-7-yl 2-(trimethylsilyl)ethyl phthalate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo301698v