Technology Process of C24H26N2O2
There total 6 articles about C24H26N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
tetrahydrofuran; methanol;
at 25 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol103022m
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere
1.2: 14 h / 25 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / 1.33 h / 0 °C / Inert atmosphere
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
3.2: -78 °C / Inert atmosphere
4.1: platinum(II) chloride / 1,4-dioxane / 24 h / Reflux; Inert atmosphere
5.1: sodium methylate / tetrahydrofuran; methanol / 0.5 h / 25 °C / Inert atmosphere
With
lithium aluminium tetrahydride; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; platinum(II) chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ol103022m
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: platinum(II) chloride / 1,4-dioxane / 24 h / Reflux; Inert atmosphere
3.1: sodium methylate / tetrahydrofuran; methanol / 0.5 h / 25 °C / Inert atmosphere
With
sodium methylate; platinum(II) chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/ol103022m
