4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

Base Information

Chemical Name:4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal
CAS No.:860437-97-4
Molecular Formula:C₃₈H₅₆O₅Si₂
Molecular Weight:649.031
Hs Code.:

4-benzyloxymethoxy-7-(<i>tert</i>-butyl-dimethyl-silanyloxy)-5-(<i>tert</i>-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

Synonyms:4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

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Chemical Property of 4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

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Technology Process of 4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

There total 3 articles about 4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 860437-99-6
C₃₉H₅₈O₄Si₂

: 860437-97-4
4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

Guidance literature:: C₃₉H₅₈O₄Si₂; With ozone; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ol0511833

Reference yield:

: 1-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxy)-5-methyl-oct-7-en-4-ol

: 860437-97-4
4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / DIPEA; tetrabutylammonium iodide / CH₂Cl₂ / 96 h

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: 96 percent / PPh₃ / CH₂Cl₂ / 5 h / 20 °C

With tetra-(n-butyl)ammonium iodide; ozone; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol0511833

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 860437-97-4
4-benzyloxymethoxy-7-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-heptanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / DIPEA; tetrabutylammonium iodide / CH₂Cl₂ / 96 h

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: 96 percent / PPh₃ / CH₂Cl₂ / 5 h / 20 °C

With tetra-(n-butyl)ammonium iodide; ozone; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol0511833