C₅₄H₇₉NO₁₇

Base Information

Chemical Name:C₅₄H₇₉NO₁₇
CAS No.:484671-55-8
Molecular Formula:C₅₄H₇₉NO₁₇
Molecular Weight:1014.22
Hs Code.:

C<sub>54</sub>H<sub>79</sub>NO<sub>17</sub>

Synonyms:C₅₄H₇₉NO₁₇

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Chemical Property of C₅₄H₇₉NO₁₇

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Technology Process of C₅₄H₇₉NO₁₇

There total 9 articles about C₅₄H₇₉NO₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 484671-54-7
C₅₄H₈₁NO₁₇

: 484671-55-8
C₅₄H₇₉NO₁₇

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 14h;
DOI:10.1021/jm051157a

Reference yield:

: 484670-62-4
C₅₅H₈₁NO₁₄

: 484671-55-8
C₅₄H₇₉NO₁₇

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridinium p-toluenesulfonate / acetonitrile; H₂O / 17 h / 68 °C

2: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO₄ / acetone; 2-methyl-propan-2-ol; H₂O / 4 h / 20 °C

3: diisopropylethylamine; (dimethylamino)pyridine / CH₂Cl₂ / 17 h / -10 °C

4: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 14 h / 0 °C

With dmap; osmium(VIII) oxide; pyridinium p-toluenesulfonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetone; acetonitrile; tert-butyl alcohol; 4: Dess-Martin oxidation;
DOI:10.1021/jm051157a

Reference yield:

: 484670-65-7
C₅₂H₇₇NO₁₄

: 484671-55-8
C₅₄H₇₉NO₁₇

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO₄ / acetone; 2-methyl-propan-2-ol; H₂O / 4 h / 20 °C

2: diisopropylethylamine; (dimethylamino)pyridine / CH₂Cl₂ / 17 h / -10 °C

3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 14 h / 0 °C

With dmap; osmium(VIII) oxide; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetone; tert-butyl alcohol; 3: Dess-Martin oxidation;
DOI:10.1021/jm051157a