3-phenylspiro

Base Information

Chemical Name:3-phenylspiro
CAS No.:100606-27-7
Molecular Formula:C₂₁H₁₃NO
Molecular Weight:295.34
Hs Code.:

3-phenylspiro<anthrone-10,2'-2'H-azirine>

Synonyms:3-phenylspiro

Suppliers and Price of 3-phenylspiro

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenylspiro

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Technology Process of 3-phenylspiro

There total 1 articles about 3-phenylspiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74975-68-1
10-(α-bromobenzylidene)anthrone

: 100606-27-7
3-phenylspiro

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1021/jo00357a027

Reference yield: 74.0%

: 2009-97-4
ethyl 2-diazo-3-oxobutanoate

: 100606-27-7
3-phenylspiro

: 1431934-90-5
ethyl 6′-methyl-10-oxo-3′-phenyl-9H-spiro[anthracene-9,2′-[1,4]-oxazine]-5′-carboxylate

Guidance literature:: With dirhodium tetraacetate; In 1,2-dichloro-ethane; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.03.106

Reference yield: 68.0%

: 884866-01-7
1-(4-methylbenzensulfonyl)-4-phenyl-1H-1,2,3-triazole

: 100606-27-7
3-phenylspiro

: 4-methyl-N-(10-oxo-2',5'-diphenyl-9H-spiro[anthracene-9,3'-pyrrol]-4'-yl)benzenesulfonamide

Guidance literature:: With dirhodium tetraacetate; In o-xylene; for 2h; Schlenk technique; Inert atmosphere; Reflux;
DOI:10.1007/s10593-018-2378-8