phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

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Chemical Name:phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside
CAS No.:928260-34-8
Molecular Formula:C₂₃H₂₅N₃O₆S
Molecular Weight:471.534
Hs Code.:

Synonyms:phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

There total 7 articles about phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-azido-2-phenyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

: 928260-34-8
phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethylformamide / 0 °C

2: p-toluenesulfonic acid hydrate / methanol / 1 h / Heating

3: 391 mg / pyridine

With pyridine; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600759

Reference yield:

: 7-azido-8-benzyloxy-2-phenyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 928260-34-8
phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid hydrate / methanol / 1 h / Heating

2: 391 mg / pyridine

With pyridine; toluene-4-sulfonic acid; In methanol;
DOI:10.1002/ejoc.200600759

Reference yield:

: 166516-71-8
phenyl 2-azido-2-deoxy-1-thio-α-D-mannopyranoside

: 928260-34-8
phenyl 4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: p-toluenesulfonic acid hydrate / acetonitrile

2: sodium hydride / dimethylformamide / 0 °C

3: p-toluenesulfonic acid hydrate / methanol / 1 h / Heating

4: 391 mg / pyridine

With pyridine; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.200600759