C₅₄H₆₃NO₇SSi

Base Information

• Chemical Name: C₅₄H₆₃NO₇SSi
• CAS No.: 1190618-80-4
• Molecular Formula: C₅₄H₆₃NO₇SSi
• Molecular Weight: 898.248
• Mol file: 1190618-80-4.mol

Synonyms:C₅₄H₆₃NO₇SSi

Chemical Property of C₅₄H₆₃NO₇SSi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₅₄H₆₃NO₇SSi

There total 1 articles about C₅₄H₆₃NO₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

C34H37NO5S (1190618-79-1) + (2S)-3-{[tert-butyl(diphenyl)silyl]oxy}-2-methylpropanal (92817-88-4) → C54H63NO7SSi (1190618-80-4)

Guidance literature:

C₃₄H₃₇NO₅S; With triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In dichloromethane; at -78 ℃; for 3.68333h; Inert atmosphere;

(2S)-3-{[tert-butyl(diphenyl)silyl]oxy}-2-methylpropanal; In dichloromethane; at -78 - 0 ℃; for 4h; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.06.144

Reference yield: 85.0%

C54H63NO7SSi (1190618-80-4) → C13H18O5 (1190618-81-5)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 8h; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.06.144

upstream raw materials:

C₃₄H₃₇NO₅S

(2S)-3-{[tert-butyl(diphenyl)silyl]oxy}-2-methylpropanal

Downstream raw materials:

C₁₃H₁₈O₅