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(S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole

Base Information Edit
  • Chemical Name:(S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole
  • CAS No.:931113-55-2
  • Molecular Formula:C21H24N4O5S
  • Molecular Weight:444.511
  • Hs Code.:
  • Mol file:931113-55-2.mol
(S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole

Synonyms:(S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole

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Chemical Property of (S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole Edit
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Technology Process of (S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole

There total 7 articles about (S)-5-(3-(2-(4-methoxyphenyl)-4-methyl-1,3-dioxolan-4-yl)propylsulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jo062513f
Guidance literature:
Multi-step reaction with 5 steps
1: 36.0 g / (DHQ)2PHAL; K3[Fe(CN)6]; K2CO3 / K2OsO2(OH)4 / 2-methyl-propan-2-ol; H2O / 48 h / 0 °C
2: PPTS / CH2Cl2 / 1.5 h / 20 °C
3: 21.77 g / TBAF / tetrahydrofuran / 2 h / cooling
4: 59 percent / Ph3P; DIAD / tetrahydrofuran / 24 h / 20 °C
5: 60 percent / MCPBA / CH2Cl2 / 16 h / 20 °C
With Hydroquinone 1,4-phthalazinediyl diether; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; potassium hexacyanoferrate(III); potassium dioxotetrahydroxoosmate(VI); In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 4: Mitsunobu reaction;
DOI:10.1021/jo062513f
Guidance literature:
Multi-step reaction with 6 steps
1: DMAP; triethylamine / CH2Cl2 / 0 - 20 °C
2: 36.0 g / (DHQ)2PHAL; K3[Fe(CN)6]; K2CO3 / K2OsO2(OH)4 / 2-methyl-propan-2-ol; H2O / 48 h / 0 °C
3: PPTS / CH2Cl2 / 1.5 h / 20 °C
4: 21.77 g / TBAF / tetrahydrofuran / 2 h / cooling
5: 59 percent / Ph3P; DIAD / tetrahydrofuran / 24 h / 20 °C
6: 60 percent / MCPBA / CH2Cl2 / 16 h / 20 °C
With dmap; Hydroquinone 1,4-phthalazinediyl diether; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; potassium hexacyanoferrate(III); potassium dioxotetrahydroxoosmate(VI); In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 5: Mitsunobu reaction;
DOI:10.1021/jo062513f
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