(3-CHLORO-5-NITROPHENYL)METHANOL

Base Information

• Chemical Name: (3-CHLORO-5-NITROPHENYL)METHANOL
• CAS No.: 79944-62-0
• Molecular Formula: C7H6 Cl N O3
• Molecular Weight: 187.583
• Hs Code.: 2906299090
• Mol file: 79944-62-0.mol

Synonyms:(3-Chloro-5-nitrophenyl)methanol;3-Chloro-5-nitrobenzenemethanol; 3-Chloro-5-nitrobenzyl alcohol

Chemical Property of (3-CHLORO-5-NITROPHENYL)METHANOL

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.612
• Boiling Point: 333.455°C at 760 mmHg
• Flash Point: 155.468°C
• PSA: 66.05000
• Density: 1.477g/cm³
• LogP: 2.26370
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(3-Chloro-5-nitrophenyl)methanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-CHLORO-5-NITROPHENYL)METHANOL

There total 6 articles about (3-CHLORO-5-NITROPHENYL)METHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(3-amino-5-nitrophenyl)methanol (90390-46-8) → (3-chloro-5-nitrophenyl)methanol (79944-62-0)

Guidance literature:

(3-amino-5-nitrophenyl)methanol; With hydrogenchloride; sodium nitrite; In water; at -5 ℃;

With hydrogenchloride; copper(l) chloride; copper dichloride; In water; at -5 - 65 ℃;

DOI:10.1016/S0040-4039(03)01270-X

Reference yield:

3-chloro-5-nitro-benzoic acid methyl ester (36138-28-0) → (3-chloro-5-nitrophenyl)methanol (79944-62-0)

Guidance literature:

3-chloro-5-nitro-benzoic acid methyl ester; With diisobutylaluminium hydride; In toluene; at -78 - 10 ℃; for 1h;

With hydrogenchloride; water; In toluene; at 0 ℃;

Reference yield:

3-chloro-5-nitrobenzoic acid (34662-36-7) → (3-chloro-5-nitrophenyl)methanol (79944-62-0)

Guidance literature:

With borane-THF; In tetrahydrofuran; at 0 - 20 ℃;

upstream raw materials:

(3-amino-5-nitrophenyl)methanol

3-chloro-5-nitro-benzoic acid methyl ester

3,5-dinitrobenzyl alcohol

3-chloro-5-nitrobenzoic acid

Downstream raw materials:

3-chloro-5-nitrobenzaldehyde

3-amino-5-chlorobenzyl alcohol

3-chloro-5-N,N-dimethylaminobenzyl alcohol

3-chloro-5-nitromandelic acid

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