(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

Base Information

Chemical Name:(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol
CAS No.:104976-43-4
Molecular Formula:C₁₄H₂₆O₉
Molecular Weight:338.355
Hs Code.:

Synonyms:(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

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Chemical Property of (2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

There total 3 articles about (2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104976-41-2
Methyl-2,3,4-tri-O-benzyl-6-O-<1D-(1,2,4/3)-2,3,4-tri-O-benzyl-1,2,3,4-tetrahydroxy-5-C-hydroxymethyl-5-cyclohexen-1-yl>-α-D-glucopyranosid

: 104976-43-4
(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 15h; under 15001.2 Torr;

Reference yield:

: 76679-47-5
methyl-2,3,4-tri-O-benzyl-6-O-trifluoromethanesulfonyl-α-D-glucopyranoside

: 104976-43-4
(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 30 min, 0 deg C; 2.) THF, 12 h, room temp.

2: 91 percent / Bu₄NF*3H₂O / tetrahydrofuran / 1 h / Ambient temperature

3: H₂ / Pd/C (10percent) / methanol / 15 h / 15001.2 Torr

With tetrabutyl ammonium fluoride; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol;

Reference yield:

: 104976-40-1
1D-(1,2,4/3)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldiphenylsilyloxy)methyl>-5-cyclohexen-1,2,3,4-tetrol

: 104976-43-4
(2S,3R,4S,5S,6R)-2-Methoxy-6-((1S,2R,3S,4R,5R)-2,3,4-trihydroxy-5-methyl-cyclohexyloxymethyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 30 min, 0 deg C; 2.) THF, 12 h, room temp.

2: 91 percent / Bu₄NF*3H₂O / tetrahydrofuran / 1 h / Ambient temperature

3: H₂ / Pd/C (10percent) / methanol / 15 h / 15001.2 Torr

With tetrabutyl ammonium fluoride; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol;