Technology Process of C11H7Cl2N3O
There total 6 articles about C11H7Cl2N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
1,2-dichloro-ethane;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: magnesium(II) chloride hexahydrate; sodium monohydrogen sulfide x-hydrate / N,N-dimethyl-formamide / 2 h / 20 °C
2: acetone / 65 °C
3: hydrazine / methanol / 20 °C
4: triethylamine / dichloromethane / 20 °C
5: acetic acid / 0.17 h / 120 °C / Microwave
6: thionyl chloride / 1,2-dichloro-ethane / Reflux
With
thionyl chloride; sodium monohydrogen sulfide x-hydrate; magnesium(II) chloride hexahydrate; acetic acid; triethylamine; hydrazine;
In
methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetone / 65 °C
2: hydrazine / methanol / 20 °C
3: triethylamine / dichloromethane / 20 °C
4: acetic acid / 0.17 h / 120 °C / Microwave
5: thionyl chloride / 1,2-dichloro-ethane / Reflux
With
thionyl chloride; acetic acid; triethylamine; hydrazine;
In
methanol; dichloromethane; 1,2-dichloro-ethane; acetone;