N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

Base Information

Chemical Name:N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide
CAS No.:781650-76-8
Molecular Formula:C₄₉H₅₀Br₂N₂O₆
Molecular Weight:922.754
Hs Code.:

Synonyms:N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

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Chemical Property of N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

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Technology Process of N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

There total 6 articles about N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 781650-75-7
(1S)-[2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl]-3-methylbutylamine

: 522647-62-7
9-(1-ethylpropyl)-1H-2-benzopyrano[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone

: 781650-76-8
N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: In N,N-dimethyl-formamide; at 155 ℃; for 24h;
DOI:10.1002/chem.200400097

Reference yield:

: 781650-73-5
2,5-dibromo-4-(2-ethylhexyloxy)phenol

: 781650-76-8
N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 36 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 20 °C

2.1: TFA / CH₂Cl₂ / 16 h / 20 °C

2.2: 91 percent / NaHCO₃ / CH₂Cl₂

3.1: 39 percent / dimethylformamide / 24 h / 155 °C

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Mitsunobu reaction;
DOI:10.1002/chem.200400097

Reference yield:

: 781650-74-6
tert-butyl [(1S)-[2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl]-3-methylbutyl]carbamate

: 781650-76-8
N-(1-ethylpropyl)-N'-[(1S)-(2,5-dibromo-4-(2-ethylhexyloxy)phenoxymethyl)-3-methylbutyl]perylene-3,4:9,10-tetracarboxylic bisimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: TFA / CH₂Cl₂ / 16 h / 20 °C

1.2: 91 percent / NaHCO₃ / CH₂Cl₂

2.1: 39 percent / dimethylformamide / 24 h / 155 °C

With trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200400097