(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

Base Information

Chemical Name:(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate
CAS No.:1440507-63-0
Molecular Formula:C₁₈H₂₃NO₃
Molecular Weight:301.386
Hs Code.:

Synonyms:(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

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Technology Process of (S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

There total 2 articles about (S)-methyl 2-benzamido-4-cyclohexylidenebutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 180470-61-5
(2S)-methyl 2-N-benzoylaminopent-4-enoate

: 1192-37-6
methylenecyclohexane

: 1440507-63-0
(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 100 ℃; for 4h; Reagent/catalyst; Temperature; Time; Microwave irradiation; Inert atmosphere;
DOI:10.1055/s-0033-1338527

Reference yield:

: 4743-91-3,72685-15-5,149117-87-3
(S)-2-benzamidopent-4-enoic acid

: 1440507-63-0
(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 18 h / 20 °C / pH 2

2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 4 h / 100 °C / Microwave irradiation; Inert atmosphere

With hydrogenchloride; Hoveyda-Grubbs catalyst second generation; In dichloromethane;
DOI:10.1055/s-0033-1338527

Reference yield: 79.0%

: 1440507-63-0
(S)-methyl 2-benzamido-4-cyclohexylidenebutanoate

: 1520942-65-7
(S)-methyl 1-benzoyl-1-azaspiro[4.5]decane-2-carboxylate

Guidance literature:: With trifluorormethanesulfonic acid; In chloroform; at 50 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1055/s-0033-1338527