ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

Base Information

Chemical Name:ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate
CAS No.:134746-26-2
Molecular Formula:C₂₃H₂₆N₂O₅
Molecular Weight:410.47
Hs Code.:

Synonyms:ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

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Chemical Property of ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

Chemical Property:

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Technology Process of ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

There total 3 articles about ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 134746-24-0
ethyl (S,R)-N-benzyloxycarbonyl-N'-(β-phenethyl)-α,α-diaminoacetate

: 814-68-6,25189-84-8
acryloyl chloride

: 134746-26-2
ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/0040-4039(91)85016-X

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 134746-26-2
ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / Et₃N / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 95 percent / Et₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With triethylamine; In dichloromethane;

Reference yield:

: 134746-23-9
ethyl 2-(((benzyloxy)carbonyl)amino)-2-chloroacetate

: 134746-26-2
ethyl (S,R)-N-benzyloxycarbonyl-N'-acryloyl-N'-(β-phenethyl)-α,α-diaminoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / Et₃N / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 95 percent / Et₃N / CH₂Cl₂ / 0.25 h / Ambient temperature

With triethylamine; In dichloromethane;