1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

Base Information

Chemical Name:1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene
CAS No.:1448461-17-3
Molecular Formula:C₁₈H₂₄O₂
Molecular Weight:272.387
Hs Code.:

Synonyms:1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

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Chemical Property of 1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

Chemical Property:

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Technology Process of 1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

There total 3 articles about 1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl (3S)-3-ethyl-2-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]pent-4-enoate

: 1448461-17-3
1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

: 1448461-29-7
1-({[(2E,4Z,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chloride; water / dimethyl sulfoxide / 7.5 h / 150 °C

2: lithium hexamethyldisilazane / toluene; 1,2-dimethoxyethane / 16 h / Sealed tube

With water; sodium chloride; lithium hexamethyldisilazane; In 1,2-dimethoxyethane; dimethyl sulfoxide; toluene; 1: |Krapcho Dealkoxycarbonylation / 2: |Julia-Kocienski Olefination;
DOI:10.1002/chem.201202822

Reference yield:

: 688317-98-8
trans-carbonic acid methyl ester pent-2-enyl ester

: 1448461-17-3
1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

: 1448461-29-7
1-({[(2E,4Z,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / tetrahydrofuran / 2.5 h / 40 °C

2: sodium chloride; water / dimethyl sulfoxide / 7.5 h / 150 °C

3: lithium hexamethyldisilazane / toluene; 1,2-dimethoxyethane / 16 h / Sealed tube

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₈H₃₄NO₄P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; water; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide; toluene; 2: |Krapcho Dealkoxycarbonylation / 3: |Julia-Kocienski Olefination;
DOI:10.1002/chem.201202822

Reference yield:

: 1448461-10-6
5-{[(2S)-2-ethylbut-3-en-1-yl]sulfonyl}-1-phenyl-1H-tetrazole

: 842125-04-6
(E)-4-((4-methoxybenzyl)oxy)but-2-en-1-al

: 1448461-17-3
1-({[(2E,4E,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

: 1448461-29-7
1-({[(2E,4Z,6S)-6-ethylocta-2,4,7-trien-1-yl]oxy}methyl)-4-methoxybenzene

Guidance literature:: With lithium hexamethyldisilazane; In 1,2-dimethoxyethane; toluene; for 16h; Reagent/catalyst; Overall yield = 93 %; Overall yield = 700 mg; Sealed tube;
DOI:10.1002/chem.201202822