(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

Base Information

Chemical Name:(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester
CAS No.:349539-82-8
Molecular Formula:C₂₀H₂₇O₆PSi
Molecular Weight:422.49
Hs Code.:

Synonyms:(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

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Chemical Property of (diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

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Technology Process of (diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

There total 2 articles about (diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 918886-60-9
benzyl (diphenylphosphono)acetate

: 349539-82-8
(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂

2: DCC; DMAP / CH₂Cl₂

With dmap; hydrogen; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(01)00436-1

Reference yield:

: 34159-52-9
2-(diphenoxyphosphoryl)acetic acid

: (2-trimethylsilanyl-ethoxy)-methanol

: 349539-82-8
(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(01)00436-1

Reference yield: 64.0%

: 349539-82-8
(diphenoxy-phosphoryl)-acetic acid 2-trimethylsilanyl-ethoxymethyl ester

: {(2R,6R)-6-[(7E,12E)-(2S,6S,10S,11S)-10-(4-Methoxy-benzyloxy)-6-methoxymethoxy-2-methyl-13-((S)-4-methyl-3,6-dihydro-2H-pyran-2-yl)-4-methylene-11-(tetrahydro-pyran-2-yloxy)-trideca-7,12-dienyl]-5,6-dihydro-2H-pyran-2-yl}-acetaldehyde

: 349539-64-6
4-{6-[10-(4-methoxy-benzyloxy)-6-methoxymethoxy-2-methyl-13-(4-methyl-3,6-dihydro-2H-pyran-2-yl)-4-methylene-11-(tetrahydro-pyran-2-yloxy)-trideca-7,12-dienyl]-5,6-dihydro-2H-pyran-2-yl}-but-2-enoic acid 2-trimethylsilanyl-ethoxymethyl ester

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1016/S0040-4039(01)00436-1