(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

Base Information

Chemical Name:(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol
CAS No.:889765-26-8
Molecular Formula:C₁₇H₃₀N₂O
Molecular Weight:278.438
Hs Code.:

Synonyms:(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

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Chemical Property of (S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

Chemical Property:

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Technology Process of (S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

There total 4 articles about (S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 889765-26-8
(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 0 - 20 °C

2: CH₂Cl₂ / Heating

3: LiAlH₄ / tetrahydrofuran / Heating

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.jorganchem.2005.04.027

Reference yield:

: N-(1-hydroxymethyl-2,2-dimethyl-propyl)-N'-(2,4,6-trimethyl-phenyl)-oxalamide

: 889765-26-8
(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;
DOI:10.1016/j.tetasy.2005.01.015 DOI:10.1016/j.jorganchem.2005.04.027

Reference yield:

: 79354-30-6
2-(2,4,6-trimethylphenylamino)-2-oxoacetic acid ethyl ester

: 889765-26-8
(S)-3,3-Dimethyl-2-[2-(2,4,6-trimethyl-phenylamino)-ethylamino]-butan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / Heating

2: LiAlH₄ / tetrahydrofuran / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2005.01.015 DOI:10.1016/j.jorganchem.2005.04.027