Technology Process of C74H104O11Si2
There total 17 articles about C74H104O11Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C34H52O7Si;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
tetrahydrofuran;
at 40 ℃;
for 2h;
Inert atmosphere;
C40H54O5Si;
With
dmap;
In
toluene;
at 40 ℃;
Inert atmosphere;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
2.1: di(n-butyl)tin oxide / methanol / 2.5 h / 70 °C / Inert atmosphere
2.2: 12 h / Inert atmosphere
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere
3.2: 40 °C / Inert atmosphere
With
2,4,6-trichlorobenzoyl chloride; diisobutylaluminium hydride; di(n-butyl)tin oxide; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
3.1: Yamaguchi esterification / 3.2: Yamaguchi esterification;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / methanol / 2.5 h / 70 °C / Inert atmosphere
1.2: 12 h / Inert atmosphere
2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere
2.2: 40 °C / Inert atmosphere
With
2,4,6-trichlorobenzoyl chloride; di(n-butyl)tin oxide; triethylamine;
In
tetrahydrofuran; methanol;
2.1: Yamaguchi esterification / 2.2: Yamaguchi esterification;
DOI:10.1021/ja200089f
