Technology Process of Carbamic acid, (1-methylcyclohexyl)-, 1,1-dimethylethyl ester (9CI)
There total 2 articles about Carbamic acid, (1-methylcyclohexyl)-, 1,1-dimethylethyl ester (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4,4,5,5-tetramethyl-2-(1-methylcyclohexyl)-1,3,2-dioxaborolane;
With
O-Methylhydroxylamin; potassium tert-butylate;
In
tetrahydrofuran; toluene;
at 80 ℃;
for 16h;
Inert atmosphere;
Sealed tube;
di-tert-butyl dicarbonate;
With
sodium hydrogencarbonate;
In
tetrahydrofuran; water; toluene;
at 20 - 80 ℃;
for 5h;
Inert atmosphere;
With
dmap;
In
water; acetonitrile;
for 1h;
Inert atmosphere;
DOI:10.1055/s-0037-1610172
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N,N-dimethyl acetamide / Inert atmosphere
1.2: Inert atmosphere
2.1: O-Methylhydroxylamin; potassium tert-butylate / tetrahydrofuran; toluene / 16 h / 80 °C / Inert atmosphere; Sealed tube
2.2: 5 h / 20 - 80 °C / Inert atmosphere
2.3: 1 h / Inert atmosphere
With
O-Methylhydroxylamin; potassium tert-butylate;
In
tetrahydrofuran; N,N-dimethyl acetamide; toluene;
DOI:10.1055/s-0037-1610172
