(+)-(3S,5R,15R,20S)-5-methylyohimbane

Base Information

Chemical Name:(+)-(3S,5R,15R,20S)-5-methylyohimbane
CAS No.:451498-78-5
Molecular Formula:C₂₀H₂₆N₂
Molecular Weight:294.44
Hs Code.:

Synonyms:(+)-(3S,5R,15R,20S)-5-methylyohimbane

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Chemical Property of (+)-(3S,5R,15R,20S)-5-methylyohimbane

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Technology Process of (+)-(3S,5R,15R,20S)-5-methylyohimbane

There total 1 articles about (+)-(3S,5R,15R,20S)-5-methylyohimbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7795-52-0,304-54-1
(-)-alpha-Methyltryptamine

: 451498-78-5
(+)-(3S,5R,15R,20S)-5-methylyohimbane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 73 percent / 2-chloro-1-methylpyridinium iodide; Bu₃N / CH₂Cl₂ / 2 h / Heating

2.1: POCl₃ / toluene / 3 h / Heating

2.2: 70 percent / NaBH₄ / methanol; H₂O

3.1: 33 percent / DIBAH / tetrahydrofuran; hexane / 18 h / 40 °C

4.1: 15 percent / NaBH₄ / methanol; H₂O

With sodium tetrahydroborate; tributyl-amine; 2-chloro-1-methyl-pyridinium iodide; diisobutylaluminium hydride; trichlorophosphate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene;
DOI:10.1002/1522-2675(200203)85:3<945::AID-HLCA945>3.0.CO;2-A