5-methyl-hex-4-enyl triphenyl phosphonium iodide

Base Information

Chemical Name:5-methyl-hex-4-enyl triphenyl phosphonium iodide
CAS No.:67858-91-7
Molecular Formula:C₂₅H₂₈P*I
Molecular Weight:486.376
Hs Code.:

Synonyms:5-methyl-hex-4-enyl triphenyl phosphonium iodide

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Chemical Property of 5-methyl-hex-4-enyl triphenyl phosphonium iodide

Chemical Property:

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Technology Process of 5-methyl-hex-4-enyl triphenyl phosphonium iodide

There total 9 articles about 5-methyl-hex-4-enyl triphenyl phosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 63588-94-3
6-iodo-2-methylhex-2-ene

: 603-35-0
triphenylphosphine

: 67858-91-7
5-methyl-hex-4-enyl triphenyl phosphonium iodide

Guidance literature:: In toluene; at 140 ℃; for 15h; Inert atmosphere;

Reference yield:

: 42272-94-6
5-methylhex-4-ene-1-ol

: 67858-91-7
5-methyl-hex-4-enyl triphenyl phosphonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: NaI / acetone

3: benzene

With triethylamine; sodium iodide; In dichloromethane; acetone; benzene;
DOI:10.1021/jo00420a003

Reference yield:

: 67859-01-2
6-methanesulfonyloxy-2-methyl-hex-2-ene

: 67858-91-7
5-methyl-hex-4-enyl triphenyl phosphonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone

2: benzene

With sodium iodide; In acetone; benzene;
DOI:10.1021/jo00420a003