Technology Process of C15H20O2
There total 3 articles about C15H20O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
p-toluenesulfonic acid monohydrate;
In
methanol;
at 0 - 20 ℃;
for 4h;
DOI:10.1002/anie.201206508
- Guidance literature:
-
Multi-step reaction with 4 steps
1: propionic acid / 23 h / 110 °C
2: lithium aluminium tetrahydride / diethyl ether / 0.33 h / -78 °C
3: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2.5 h / 0 °C
4: p-toluenesulfonic acid monohydrate / methanol / 4 h / 0 - 20 °C
With
lithium aluminium tetrahydride; p-toluenesulfonic acid monohydrate; sodium hydride; propionic acid;
In
methanol; diethyl ether; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201206508
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 2.5 h / 0 °C
2: p-toluenesulfonic acid monohydrate / methanol / 4 h / 0 - 20 °C
With
p-toluenesulfonic acid monohydrate; sodium hydride;
In
methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201206508