4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

Base Information

Chemical Name:4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide
CAS No.:152793-31-2
Molecular Formula:C₂₈H₂₀N₄O₅
Molecular Weight:492.491
Hs Code.:

Synonyms:4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

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Chemical Property of 4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

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Technology Process of 4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

There total 5 articles about 4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 152793-27-6
4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine

: 152793-31-2
4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/hlca.19930760323

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 152793-31-2
4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / NaOEt / ethanol / 1 h / Heating

2: 88 percent / NaOH / ethanol; tetrahydrofuran; H₂O / 5 h / Ambient temperature

3: 57 percent / AcONH₄ / methanol / 24 h / Heating

4: 84 percent / 3-chloroperbenzoic acid / CH₂Cl₂

With sodium hydroxide; ammonium acetate; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19930760323

Reference yield:

: 152793-23-2
4-(3-nitro benzyloxy) benzaldehyde

: 152793-31-2
4'-<4'''-(3''''-Nitrobenzyloxy)phenyl>-2,2':6',2''-terpyridine N,N''-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NaOH / ethanol; tetrahydrofuran; H₂O / 5 h / Ambient temperature

2: 57 percent / AcONH₄ / methanol / 24 h / Heating

3: 84 percent / 3-chloroperbenzoic acid / CH₂Cl₂

With sodium hydroxide; ammonium acetate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19930760323