Technology Process of C26H27ClN6O3
There total 9 articles about C26H27ClN6O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C
2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C
3: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; caesium carbonate; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N,N,N,-tetramethylethylenediamine; lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere
1.2: 0.5 h / 60 °C
2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C
3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
With
N,N,N,N,-tetramethylethylenediamine; caesium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;