ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate

Base Information

• Chemical Name: ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate
• CAS No.: 113370-82-4
• Molecular Formula: C₂₁H₂₀N₂O₄
• Molecular Weight: 364.401

Synonyms:ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate

Chemical Property of ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate

Chemical Property:

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Technology Process of ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate

There total 2 articles about ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-phenyl-maleimide (941-69-5) + [(benzylidene)amino]acetic acid ethyl ester (133038-44-5) → ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate (113370-82-4)

Guidance literature:

In toluene; for 48h; Heating;

DOI:10.1039/P19870002285

Reference yield:

N-phenyl-maleimide (941-69-5) + ethyl 2-(benzylimino)acetate (64222-28-2) → ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate (113370-82-4)

Guidance literature:

With silver(I) acetate; triethylamine; In acetonitrile; at 20 ℃; for 24h; Solvent; Reagent/catalyst; stereoselective reaction;

DOI:10.1021/ol5022614

Reference yield: 99.0%

ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>octane-2-carboxylate (113370-82-4) → ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>oct-3-ene-2-carboxylate (113371-31-6)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; 25 deg C, 24 h, 80 deg C, 1 h;

DOI:10.1039/P19870002285

upstream raw materials:

N-phenyl-maleimide

[(benzylidene)amino]acetic acid ethyl ester

ethyl 2-(benzylimino)acetate

Downstream raw materials:

ethyl 6,8-dioxo-4,7-diphenyl-3,7-diazabicyclo<3.3.0>oct-3-ene-2-carboxylate

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