Technology Process of (1R,2S,3R)-3-O-benzyl-1,2,3-cyclohexanetriol
There total 5 articles about (1R,2S,3R)-3-O-benzyl-1,2,3-cyclohexanetriol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 94 percent / boron trifluoride etherate / CHCl3 / 3 h / Ambient temperature
2: 95 percent / conc. sulfuric acid / dimethylformamide / 24 h / Ambient temperature
3: 95 percent / sodium hydride dispersion (50percent in oil) / dimethylformamide / 4 h / Ambient temperature
4: 90 percent / acetic acid, water / 3 h / Heating
5: 70 percent / ethanol / Raney-Nickel / 12 h / Heating
With
ethanol; sulfuric acid; boron trifluoride diethyl etherate; water; sodium hydride; acetic acid;
nickel;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660127
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / conc. sulfuric acid / dimethylformamide / 24 h / Ambient temperature
2: 95 percent / sodium hydride dispersion (50percent in oil) / dimethylformamide / 4 h / Ambient temperature
3: 90 percent / acetic acid, water / 3 h / Heating
4: 70 percent / ethanol / Raney-Nickel / 12 h / Heating
With
ethanol; sulfuric acid; water; sodium hydride; acetic acid;
nickel;
In
N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660127
