5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

Base Information

Chemical Name:5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine
CAS No.:267661-98-3
Molecular Formula:C₅₂H₆₀N₄O₁₈
Molecular Weight:1029.06
Hs Code.:

Synonyms:5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

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Chemical Property of 5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

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Technology Process of 5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

There total 1 articles about 5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 183660-36-8
Acetic acid (1S,2S,3R,4S,6R)-4,6-bis-benzyloxycarbonylamino-3-[(2R,3R,4R,5R,6R)-4,5-diacetoxy-3-benzyloxycarbonylamino-6-(benzyloxycarbonylamino-methyl)-tetrahydro-pyran-2-yloxy]-2-(2-oxo-ethoxy)-cyclohexyl ester

: 267661-98-3
5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

Guidance literature:: With sodium tris(acetoxy)borohydride; In benzene; for 3h; Heating;
DOI:10.1080/15257770008033010

Reference yield: 49.0%

: 267661-99-4
1-O-acetyl-5-acetylamino-2,3-di-O-benzoyl-5-deoxy-α,β-D-ribofuranose

: 267661-98-3
5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

: 4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonyl-5-O-[ethyl-2-(5-deoxy-5-trifluoroacetylamino-2,3-di-O-benzoyl-β-D-ribofuranosidyl)]neamine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1080/15257770008033010

Reference yield: 37.0%

: 1-O-acetyl-6-azido-6-deoxy-2,3,4-tri-O-benzyl-α,β-D-glycopyranoside

: 267661-98-3
5-O-hydroxyethyl-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

: 5-O-[ethyl-2-(6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-glycopyranosidyl)]-4,3',4'-tri-O-acetyl-1,3,2',6'-tetra-N-benzyloxycarbonylneamine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1080/15257770008033010