9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

Base Information

Chemical Name:9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate
CAS No.:371226-24-3
Molecular Formula:C₃₀H₄₁N₃O₅
Molecular Weight:523.673
Hs Code.:

Synonyms:9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

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Chemical Property of 9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

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Technology Process of 9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

There total 6 articles about 9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 221161-37-1
4-(tert-butoxyformamido)phenethyl chloride

: 371226-28-7
O-(9-azabicyclo[3.3.1]nonan-3α-yl)-N-(2-methoxy-5-methylphenyl)carbamate

: 371226-24-3
9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; for 48h; Heating;

Reference yield:

: 363140-31-2
N-(9-benzyl-9-azabicyclo[3.3.1]nonan-3α-yl)-N'-(2-methoxy-5-methylphenyl)carbamate

: 371226-24-3
9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol

2: 38 percent / potassium iodide; potassium carbonate / acetonitrile / 48 h / Heating

With hydrogen; potassium carbonate; potassium iodide; palladium on activated charcoal; In ethanol; acetonitrile;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 371226-24-3
9-[(4-tert-butoxyformamido)phenethyl]-9-azabicyclo[3.3.1]nonan-3α-yl N-(2-methoxy-5-methylphenyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / ethyl acetate / 48 h / 20 °C

2: 95 percent / triphenyl phosphine; carbon tetrachloride / 24 h / Heating

3: 38 percent / potassium iodide; potassium carbonate / acetonitrile / 48 h / Heating

With tetrachloromethane; potassium carbonate; triphenylphosphine; potassium iodide; In ethyl acetate; acetonitrile;