C₂₀H₁₄⁽²⁾H₄ClNO₆

Base Information

• Chemical Name: C₂₀H₁₄⁽²⁾H₄ClNO₆
• CAS No.: 1448049-52-2
• Molecular Formula: C₂₀H₁₈ClNO₆
• Molecular Weight: 407.787
• Mol file: 1448049-52-2.mol

Synonyms:C₂₀H₁₄⁽²⁾H₄ClNO₆

Chemical Property of C₂₀H₁₄⁽²⁾H₄ClNO₆

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₀H₁₄⁽²⁾H₄ClNO₆

There total 6 articles about C₂₀H₁₄⁽²⁾H₄ClNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H22(2)H4ClNO6 → C20H14(2)H4ClNO6 (1448049-50-0) + C20H14(2)H4ClNO6 (1448049-52-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ol401630t

Reference yield:

C13H10(2)H4O5 (1496506-67-2) → C20H14(2)H4ClNO6 (1448049-50-0) + C20H14(2)H4ClNO6 (1448049-52-2)

Guidance literature:

Multi-step reaction with 5 steps

1: sulfuryl dichloride / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: lithium hydroxide / ethanol; water / 1 h / Reflux

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

4: N,N-dimethyl-formamide; triethylamine / dichloromethane / 0.25 h

5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With sulfuryl dichloride; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; lithium hydroxide; In ethanol; dichloromethane; water;

DOI:10.1021/ol401630t

Reference yield:

C13H9(2)H4ClO5 → C20H14(2)H4ClNO6 (1448049-50-0) + C20H14(2)H4ClNO6 (1448049-52-2)

Guidance literature:

Multi-step reaction with 4 steps

1: lithium hydroxide / ethanol; water / 1 h / Reflux

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane

3: N,N-dimethyl-formamide; triethylamine / dichloromethane / 0.25 h

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; lithium hydroxide; In ethanol; dichloromethane; water;

DOI:10.1021/ol401630t

upstream raw materials:

C₁₃H₁₀⁽²⁾H₄O₅

C₁₁H₅⁽²⁾H₄ClO₅