Technology Process of pentadecan-1,12-diol
There total 4 articles about pentadecan-1,12-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
for 1h;
DOI:10.1021/ol035254e
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 54 percent / I2 / CH2Cl2
2: 88 percent / sodium acetate; PCC / CH2Cl2
3: 100 percent / diethyl ether / -40 °C
4: 94 percent / p-toluenesulfonic acid / methanol / 1 h
With
iodine; sodium acetate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
methanol; diethyl ether; dichloromethane;
3: Grignard reaction;
DOI:10.1021/ol035254e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / sodium acetate; PCC / CH2Cl2
2: 100 percent / diethyl ether / -40 °C
3: 94 percent / p-toluenesulfonic acid / methanol / 1 h
With
sodium acetate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
methanol; diethyl ether; dichloromethane;
2: Grignard reaction;
DOI:10.1021/ol035254e
