C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)

Base Information

Chemical Name:C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)
CAS No.:85454-61-1
Molecular Formula:C₃₁H₂₉CoNOP
Molecular Weight:521.544
Hs Code.:

C<sub>5</sub>H<sub>5</sub>Co(P(C<sub>6</sub>H<sub>5</sub>)3)(CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>NO)

Synonyms:C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)

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Chemical Property of C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)

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Technology Process of C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)

There total 1 articles about C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 78305-62-1
Na⁽¹⁺⁾*Co(C₅H₅)NO^(1-)=NaCo(C₅H₅)NO

: 104-81-4
4-Methylbenzyl bromide

: 85454-61-1
C₅H₅Co(P(C₆H₅)3)(CH₃C₆H₄CH₂NO)

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; byproducts: NaBr; benzyl bromide adding with stirring to a soln. of Co complex in THF under N2, after 1 min PPh3 adding, stirring for 8 h, solvent removing in vacuo, CH2Cl2 adding, NaBr filtering off, evapg.; purified by recrystn. from pentane/CH2Cl2 at -40°C; identified by elem. anal., IR and NMR spectra;
DOI:10.1021/ja00350a030