benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

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Chemical Name:benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate
CAS No.:1392224-83-7
Molecular Formula:C₉₉H₁₁₇Cl₃N₂O₂₇Si
Molecular Weight:1901.46
Hs Code.:

benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

Synonyms:benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

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Chemical Property of benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

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Technology Process of benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

There total 1 articles about benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1392224-82-6
benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-amino-propyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-mannooctulopyranosid]onate

: 1392224-83-7
benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

Guidance literature:: With ethanol; hydrazinium monoacetate; In toluene; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja306274v

Reference yield: 82.0%

: 1392224-83-7
benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-aminopropyl-4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

: 1392224-69-9
C₃₀H₂₈F₃NO₇

: 1392224-84-8
benzyl 3-O-acetyl-2-deoxy-2-(2,2,2-trichloroethyloxycarbonyl)-amino-4,6-O-(di-tert-butylsilanediyl)-α-D-galactosamine-(1→2)-4,6-di-O-benzylidene-3-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-O-[2-O-acetyl-3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranosyl-(1→2)]-α-D-mannopyranosyl-(1→5)-[N-benzyloxycarbonyl-3-amino-propyl 4-O-benzyl-3-deoxy-7,8-O-isopropylidene-α-D-manno-octulopyranosid]onate

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja306274v