2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

Base Information

Chemical Name:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester
CAS No.:86802-59-7
Molecular Formula:C₂₄H₃₀N₂O₈
Molecular Weight:474.511
Hs Code.:

Synonyms:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

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Chemical Property of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

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Technology Process of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

There total 5 articles about 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 39562-25-9
3-oxo-2-(3-nitrophenylmethylene)butanoic acid isopropyl ester

: 86780-83-8
3,3-ethylenedioxybutyl 3-aminocrotonate

: 86802-59-7
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

Guidance literature:: In ethanol; Heating;
DOI:10.1248/cpb.34.1589

Reference yield:

: 5754-32-5
2-(2-methyl-1,3-dioxolan-2-yl)ethanol

: 86802-59-7
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 60percent NaH in oil / 2 h / 70 - 80 °C

2: 87 percent / NH₃ / methanol / 4 h / 0 - 5 °C

3: 85 percent / ethanol / Heating

With ammonia; sodium hydride; In methanol; ethanol;
DOI:10.1248/cpb.34.1589

Reference yield:

: 542-08-5
isopropyl acetoacetate

: 86802-59-7
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-isopropyl ester 5-[2-(2-methyl-[1,3]dioxolan-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / AcOH, piperidine / benzene / 4 h / Ambient temperature

2: 85 percent / ethanol / Heating

With piperidine; acetic acid; In ethanol; benzene;
DOI:10.1248/cpb.34.1589