(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

Base Information

Chemical Name:(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate
CAS No.:1172140-56-5
Molecular Formula:C₂₁H₂₃NO₄
Molecular Weight:353.418
Hs Code.:

Synonyms:(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

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Chemical Property of (3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

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Technology Process of (3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

There total 1 articles about (3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1172140-58-7
C₁₃H₁₇NO₂

: 501-53-1,94274-21-2
benzyl chloroformate

: 1172140-56-5
(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

Guidance literature:: C₁₃H₁₇NO₂; With sodium carbonate; In tetrahydrofuran; diethyl ether; water; for 0.333333h;

benzyl chloroformate; In tetrahydrofuran; diethyl ether; water; at 12 ℃; for 1.25h;

Reference yield:

: 1172140-56-5
(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

: 1172140-58-7
C₁₃H₁₇NO₂

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2.25h; Inert atmosphere; Cooling;

Reference yield:

: 1172140-56-5
(3R,3aR,6S,6aR)-benzyl 6-benzyl-3-hydroxytetrahydro-2H-furo[3,2-b]pyrrole-4(5H)-carboxylate

: 1172140-59-8
(3aS,6S,6aR)-(9H-fluoren-9-yl)methyl 6-benzyl-3-oxotetrahydro-2H-furo[3.2-b]pyrrole-4(5H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / Cooling with ice

2: sodium carbonate / 1,4-dioxane; water / 0 °C

3: Dess-Martin periodane / dichloromethane / 2 h / Inert atmosphere

With hydrogen; sodium carbonate; Dess-Martin periodane; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; water;