C₂₉H₂₆BrIO₆

Base Information

Chemical Name:C₂₉H₂₆BrIO₆
CAS No.:1311379-32-4
Molecular Formula:C₂₉H₂₆BrIO₆
Molecular Weight:677.33
Hs Code.:

C<sub>29</sub>H<sub>26</sub>BrIO<sub>6</sub>

Synonyms:C₂₉H₂₆BrIO₆

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Chemical Property of C₂₉H₂₆BrIO₆

Chemical Property:

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Technology Process of C₂₉H₂₆BrIO₆

There total 11 articles about C₂₉H₂₆BrIO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1311379-29-9
C₂₂H₂₃IO₅

: 586-75-4
4-chlorobenzoyl chloride

: 1311379-32-4
C₂₉H₂₆BrIO₆

Guidance literature:: C₂₂H₂₃IO₅; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;

4-chlorobenzoyl chloride; In N,N-dimethyl-formamide; mineral oil; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja203642n

Reference yield:

: 1311379-26-6
C₁₅H₁₈O₅

: 1311379-32-4
C₂₉H₂₆BrIO₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

4.1: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere

5.2: 1 h / 60 °C / Inert atmosphere

With chloro-trimethyl-silane; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; mineral oil; 4.1: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₄

: 1311379-32-4
C₂₉H₂₆BrIO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

2.1: sulfuric acid / 0 - 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

4.1: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

6.1: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / Inert atmosphere

7.2: 1 h / 60 °C / Inert atmosphere

With sodium chlorite; chloro-trimethyl-silane; sodium phosphate monobasic monohydrate; sulfuric acid; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 2-methyl-but-2-ene; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: Pinnick oxidation / 6.1: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n