4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

Base Information

Chemical Name:4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside
CAS No.:1352627-53-2
Molecular Formula:C₁₈H₂₂O₈S
Molecular Weight:398.434
Hs Code.:

Synonyms:4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

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Chemical Property of 4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

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Technology Process of 4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

There total 2 articles about 4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₈O₆S

: 1352627-53-2
4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

Guidance literature:: With pyridine; acetic anhydride; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c1ob06227a

Reference yield:

: 461666-79-5
4'-methoxyphenyl α-L-arabinofuranoside

: 1352627-53-2
4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling

2: pyridine; acetic anhydride / 3 h / 20 °C / Inert atmosphere

With pyridine; di-isopropyl azodicarboxylate; acetic anhydride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1039/c1ob06227a

Reference yield: 98.0%

: 1352627-53-2
4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside

: 1352627-58-7
4'-methoxyphenyl 5-deoxy-5-thio-α-L-arabinofuranoside

Guidance literature:: 4'-methoxyphenyl 2,3-di-O-acetyl-5-deoxy-5-thioacetyl-α-L-arabinofuranoside; With sodium methylate; In methanol; at 20 ℃;

In methanol;
DOI:10.1039/c1ob06227a