(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

Base Information

Chemical Name:(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride
CAS No.:253316-00-6
Molecular Formula:C₁₅H₁₆ClNOS
Molecular Weight:293.817
Hs Code.:

Synonyms:(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

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Chemical Property of (S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

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Technology Process of (S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

There total 5 articles about (S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37754-48-6
(R,S_S)-N-α-methylbenzyl-p-tolylsulfinamide

: 253316-00-6
(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

Guidance literature:: With tert-butylhypochlorite; In tetrachloromethane; at 0 ℃; for 1h;
DOI:10.1080/10426509908037031

Reference yield:

: 10439-23-3
4-methylbenzenesulfinyl chloride

: 253316-00-6
(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1 h / 25 °C

2: t-BuOCl / CCl₄ / 1 h / 0 °C

With tert-butylhypochlorite; In tetrachloromethane; diethyl ether; 1: Substitution / 2: Chlorination;
DOI:10.1080/10426509908037031

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 253316-00-6
(S)-N-[(R)-1-phenylethyl]-p-toluenesulfonimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / diethyl ether; hexane / 0.25 h / 0 °C

1.2: 89 percent / diethyl ether; hexane / 1 h / 0 °C

2.1: t-BuOCl / CCl₄ / 1 h / 0 °C

With n-butyllithium; tert-butylhypochlorite; In tetrachloromethane; diethyl ether; hexane; 1.1: deprotonation / 1.2: Substitution / 2.1: Chlorination;
DOI:10.1080/10426509908037031