C₁₇H₂₀BrNO₄

Base Information

Chemical Name:C₁₇H₂₀BrNO₄
CAS No.:1311410-89-5
Molecular Formula:C₁₇H₂₀BrNO₄
Molecular Weight:382.254
Hs Code.:

C<sub>17</sub>H<sub>20</sub>BrNO<sub>4</sub>

Synonyms:C₁₇H₂₀BrNO₄

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Chemical Property of C₁₇H₂₀BrNO₄

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Technology Process of C₁₇H₂₀BrNO₄

There total 4 articles about C₁₇H₂₀BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: C₁₇H₂₀BrNO₄

: 1311410-89-5
C₁₇H₂₀BrNO₄

: C₁₇H₂₀BrNO₄

Guidance literature:: With Chiralpak Daicel AD-20; In isopropyl alcohol; Resolution of racemate;

Reference yield:

: 1311410-86-2
C₁₉H₂₂BrNO₄S

: 1311410-89-5
C₁₇H₂₀BrNO₄

: C₁₇H₂₀BrNO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C

1.3: -40 °C

2.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

With n-butyllithium; diisopropylamine; In tetrahydrofuran; isopropyl alcohol;

Reference yield:

: 4654-39-1
4-bromophenethanol

: 1311410-89-5
C₁₇H₂₀BrNO₄

: C₁₇H₂₀BrNO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate; sodium hypochlorite; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0 °C

2.1: formic acid / water; methanol / 24 h / 40 °C

3.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.33 h / -78 °C

3.3: -40 °C

4.1: Chiralpak Daicel^.(R). AD-20 / isopropyl alcohol / Resolution of racemate

With sodium hypochlorite; n-butyllithium; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; diisopropylamine; sodium bromide; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;