Technology Process of C30H53N2O7P
There total 4 articles about C30H53N2O7P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H36N2O4;
With
1H-tetrazole;
In
tetrahydrofuran; dichloromethane;
for 0.5h;
di-tert-butyl diisopropylphosphoramide;
In
tetrahydrofuran; dichloromethane;
for 15h;
With
dihydrogen peroxide;
In
tetrahydrofuran; dichloromethane;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide; N-ethyl-N,N-diisopropylamine; triphenylphosphine / bis(dibenzylideneacetone)-palladium(0) / tetrahydrofuran / 12 h / 20 °C
2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h
2.2: 4 h
3.1: hydrogen / palladium on activated charcoal / ethanol / 12 h
4.1: 1H-tetrazole / tetrahydrofuran; dichloromethane / 0.5 h
4.2: 15 h
4.3: 24 h
With
1H-tetrazole; copper(l) iodide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
palladium on activated charcoal; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogen / palladium on activated charcoal / ethanol / 12 h
2.1: 1H-tetrazole / tetrahydrofuran; dichloromethane / 0.5 h
2.2: 15 h
2.3: 24 h
With
1H-tetrazole; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane;
