ferrocenoic thioanhydride

Base Information

Chemical Name:ferrocenoic thioanhydride
CAS No.:63118-92-3
Molecular Formula:C₂₂H₁₈Fe₂O₂S
Molecular Weight:458.144
Hs Code.:

Synonyms:ferrocenoic thioanhydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ferrocenoic thioanhydride

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Technology Process of ferrocenoic thioanhydride

There total 1 articles about ferrocenoic thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 226882-93-5
ferrocene carboxylic acid fluoride

: 140-89-6
potassium ethyl xanthogenate

: 1271-42-7
ferrocenecarboxylic acid

: 63118-92-3
ferrocenoic thioanhydride

Guidance literature:: With dmap; In neat (no solvent); ferrocenyl fluoride, potassium-O-ethyl xanthate, N,N-dimethylaminopyridine were mixed and ground in the dark for 3 min; mixt. was taken up in min. amt. of CH2Cl2; subjected to column chromy. using hexane-Et2O (1:3) as eluent; solvent removed (vac.); ferrocenemonocarboxylic acid was stripped off the column with MeOH;
DOI:10.1016/j.jorganchem.2005.08.015