(2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate

Base Information

• Chemical Name: (2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate
• CAS No.: 1054608-41-1
• Molecular Formula: C₃₀H₅₄O₇Si₂
• Molecular Weight: 582.926

Synonyms:(2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate

Chemical Property of (2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate

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Technology Process of (2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate

There total 1 articles about (2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2R,3R,4R)-methyl-2-(2-(benzyloxy)-3,5-dimethoxy-4-methylphenyl)-4-hydroxy-3,5-dimethyl-3,4-dihydro-2H-pyran-6-carboxylate (1054608-40-0) + t-butyldimethylsiyl triflate (69739-34-0) → (2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate (1054608-41-1)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol801499s

Reference yield: 90.0%

(2S,3S,4R,5S,6R)-methyl-4-(tert-butyldimethylsilyloxy)-6-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate (1054608-41-1) → (2S,3S,4R,5S,6R)-methyl-6-(2-bromo-6-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-4-(tert-butyldimethylsilyloxy)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate (1054608-63-7)

Guidance literature:

With bromine; methyloxirane; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol801499s

upstream raw materials:

(2R,3R,4R)-methyl-2-(2-(benzyloxy)-3,5-dimethoxy-4-methylphenyl)-4-hydroxy-3,5-dimethyl-3,4-dihydro-2H-pyran-6-carboxylate

t-butyldimethylsiyl triflate

Downstream raw materials:

(2S,3S,4R,5S,6R)-methyl-6-(2-bromo-6-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-4-methylphenyl)-4-(tert-butyldimethylsilyloxy)-3,5-dimethyltetrahydro-2H-pyran-2-carboxylate

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