3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

Base Information

Chemical Name:3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene
CAS No.:921229-81-4
Molecular Formula:C₃₆H₆₅IO₃
Molecular Weight:672.815
Hs Code.:

Synonyms:3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

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Chemical Property of 3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

Chemical Property:

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Technology Process of 3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

There total 6 articles about 3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)benzenediazonium tetrafluoroborate

: 921229-81-4
3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

Guidance literature:: With 18-crown-6 ether; iodine; potassium acetate; In chloroform;
DOI:10.1021/ja0665848

Reference yield:

: 921229-75-6
1,2,3-tris((S)-3,7-dimethyloctan-1-yloxy)benzene

: 921229-81-4
3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / silica gel-supported nitric acid / CH₂Cl₂ / 0.08 h

2: 94 percent / hydrazine monohydrate; graphite / ethanol / 12 h / Heating

3: 90 percent / aq. HBF₄; t-butyl nitrite / CH₂Cl₂; tetrahydrofuran / 10 - 15 °C

4: 90 percent / potassium acetate; 18-crown-6; I₂ / CHCl₃

With tetrafluoroboric acid; tert.-butylnitrite; 18-crown-6 ether; iodine; nitric acid; potassium acetate; silica gel; pyrographite; hydrazine hydrate; In tetrahydrofuran; ethanol; dichloromethane; chloroform;
DOI:10.1021/ja0665848

Reference yield:

: 921229-76-7
3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-nitrobenzene

: 921229-81-4
3,4,5-tris((S)-3,7-dimethyloctan-1-yloxy)-1-iodobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / hydrazine monohydrate; graphite / ethanol / 12 h / Heating

2: 90 percent / aq. HBF₄; t-butyl nitrite / CH₂Cl₂; tetrahydrofuran / 10 - 15 °C

3: 90 percent / potassium acetate; 18-crown-6; I₂ / CHCl₃

With tetrafluoroboric acid; tert.-butylnitrite; 18-crown-6 ether; iodine; potassium acetate; pyrographite; hydrazine hydrate; In tetrahydrofuran; ethanol; dichloromethane; chloroform;
DOI:10.1021/ja0665848