(5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

Base Information

Chemical Name:(5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate
CAS No.:1027086-68-5
Molecular Formula:C₃₂H₅₀O₆Si₂
Molecular Weight:586.916
Hs Code.:

Synonyms:(5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

Suppliers and Price of (5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

There total 1 articles about (5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1027086-66-3
(R)-1-methoxy-4-(((2-methylbut-3-yn-1-yl)oxy)methyl)benzene

: 1027086-54-9
(5S,6S)-methyl 6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)nona-2,8-diynoate

: 1027086-68-5
(5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

Guidance literature:: With palladium diacetate; tris(2,6-dimethoxyphenyl)phosphine; In benzene; at 20 ℃; for 10.5h;
DOI:10.1021/ol800347u

Reference yield: 60.0%

: 1027086-68-5
(5S,6S,E)-methyl 3-((R)-4-(4-methoxybenzyloxy)-3-methylbut-1-ynyl)-6-(tert-butyldimethylsilyloxy)-5-hydroxy-9-(trimethylsilyl)non-2-en-8-ynoate

: 1027086-70-9
(E)-methyl 2-((S)-6-((S)-1-(4-methoxybenzyloxy)propan-2-yl)-2-((S)-1-(tert-butyldimethylsilyloxy)-4-(trimethylsilyl)but-3-ynyl)-2,3-dihydropyran-4-ylidene)acetate

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); tris(2,6-dimethoxyphenyl)phosphine; In tetrahydrofuran; at 20 ℃; for 2.5h;
DOI:10.1021/ol800347u