1,3-bis(methoxymethoxy)-5-vinylbenzene

Base Information

• Chemical Name: 1,3-bis(methoxymethoxy)-5-vinylbenzene
• CAS No.: 1438867-27-6
• Molecular Formula: C₁₂H₁₆O₄
• Molecular Weight: 224.257

Synonyms:1,3-bis(methoxymethoxy)-5-vinylbenzene

Chemical Property of 1,3-bis(methoxymethoxy)-5-vinylbenzene

Chemical Property:

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Technology Process of 1,3-bis(methoxymethoxy)-5-vinylbenzene

There total 4 articles about 1,3-bis(methoxymethoxy)-5-vinylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3,5-di-[(methoxymethyl)oxy]benzaldehyde (76280-61-0) → 1,3-bis(methoxymethoxy)-5-vinylbenzene (1438867-27-6)

Guidance literature:

With Methyltriphenylphosphonium bromide; sodium hydride; In tetrahydrofuran; mineral oil; at 65 ℃; Inert atmosphere;

DOI:10.1039/c3ob40420j

Reference yield:

[3,5-bis(methoxymethoxy)phenyl]methanol (76280-60-9) → 1,3-bis(methoxymethoxy)-5-vinylbenzene (1438867-27-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

2: Methyltriphenylphosphonium bromide; sodium hydride / tetrahydrofuran; mineral oil / 65 °C / Inert atmosphere

With Methyltriphenylphosphonium bromide; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; mineral oil;

DOI:10.1039/c3ob40420j

Reference yield:

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) → 1,3-bis(methoxymethoxy)-5-vinylbenzene (1438867-27-6)

Guidance literature:

Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 6 h / 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

4: Methyltriphenylphosphonium bromide; sodium hydride / tetrahydrofuran; mineral oil / 65 °C / Inert atmosphere

With lithium aluminium tetrahydride; Methyltriphenylphosphonium bromide; sodium hydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; mineral oil;

DOI:10.1039/c3ob40420j

upstream raw materials:

3,5-di-[(methoxymethyl)oxy]benzaldehyde

methyl 3,5-bis(methoxymethoxy)benzoate

[3,5-bis(methoxymethoxy)phenyl]methanol

1-carbomethoxy-3,5-dihydroxybenzene

Downstream raw materials:

(E)-1,3-bis(methoxymethoxy)-5-(4-methoxystyryl)-benzene

(E)-4-(3,5-bis(methoxymethoxy)styryl)phenol

(E)-5-[2-4-(hydroxyphenyl)ethenyl]-1,3-benzenediol

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