2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

Base Information

Chemical Name:2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine
CAS No.:1027412-56-1
Molecular Formula:C₄₃H₃₈ClN₅
Molecular Weight:660.261
Hs Code.:

Synonyms:2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

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Chemical Property of 2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

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Technology Process of 2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

There total 18 articles about 2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 153806-49-6
2-butyl-6-chloro-4-methyl-3-<<2'-(triphenylmethyltetrazol-5-yl)biphenyl-4-yl>chloromethyl>pyridine

: 1027412-56-1
2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

Guidance literature:: With acetic acid; zinc; for 0.583333h; Ambient temperature;
DOI:10.1248/cpb.42.1841

Reference yield:

: 74697-23-7
ethyl-3-aminohept-2-enoate

: 1027412-56-1
2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

Guidance literature:: Multi-step reaction with 9 steps

1: piperidine / ethanol / 3 h / Heating

2: 1 N aq. (NH₄)2Ce(NO₃)6 / acetone / 0.33 h / 0 °C

3: 73.7 percent / m-chloroperbenzoic acid / CHCl₃ / 4 h / Ambient temperature

4: 42.7 percent / POCl₃ / 2 h / Heating

5: 82.9 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

6: 87.8 percent / MnO₂ / CHCl₃ / 5 h / Heating

7: 1.) Mg / 1.) THF, 2.) THF, -78 deg C, 1.5 h

8: 85 percent / SOCl₂ / 0.5 h / 60 °C

9: 100 percent / Zn, AcOH / 0.58 h / Ambient temperature

With piperidine; manganese(IV) oxide; lithium aluminium tetrahydride; thionyl chloride; ammonium cerium(IV) nitrate; magnesium; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; trichlorophosphate; In tetrahydrofuran; ethanol; chloroform; acetone;
DOI:10.1248/cpb.42.1841

Reference yield:

: 1027843-56-6
(2-Butyl-6-chloro-4-methyl-pyridin-3-yl)-methanol

: 1027412-56-1
2-Butyl-6-chloro-4-methyl-3-[2'-(1-trityl-1H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 87.8 percent / MnO₂ / CHCl₃ / 5 h / Heating

2: 1.) Mg / 1.) THF, 2.) THF, -78 deg C, 1.5 h

3: 85 percent / SOCl₂ / 0.5 h / 60 °C

4: 100 percent / Zn, AcOH / 0.58 h / Ambient temperature

With manganese(IV) oxide; thionyl chloride; magnesium; acetic acid; zinc; In chloroform;
DOI:10.1248/cpb.42.1841