C₃₃H₄₀N₂O₆

Base Information

Chemical Name:C₃₃H₄₀N₂O₆
CAS No.:362517-19-9
Molecular Formula:C₃₃H₄₀N₂O₆
Molecular Weight:560.69
Hs Code.:

C<sub>33</sub>H<sub>40</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₃H₄₀N₂O₆

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Chemical Property of C₃₃H₄₀N₂O₆

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Technology Process of C₃₃H₄₀N₂O₆

There total 9 articles about C₃₃H₄₀N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362517-09-7
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2S)-2-ethyl-2,3-(isopropylidenedioxy)propyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362517-19-9
C₃₃H₄₀N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

2.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

3.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

4.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

4.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

5.1: thiocresol / 2 h / 110 °C

5.2: 2.458 g / tributyltin hydride; 2,2'-azobisisobutyronitrile / toluene / 24 h / Heating

With dmap; p-toluenesulfonylanhydride; ammonium formate; diisobutylaluminium hydride; sodium hydrogencarbonate; triethylamine; para-thiocresol; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1021/jo000250y

Reference yield:

: 362517-06-4
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2R)-2-ethyl-2,3-epoxypropyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362517-19-9
C₃₃H₄₀N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 13.6 percent / sulfuric acid/silica gel; water / dioxane / 0.17 h

2.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

3.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

4.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

5.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

5.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

6.1: thiocresol / 2 h / 110 °C

6.2: 2.458 g / tributyltin hydride; 2,2'-azobisisobutyronitrile / toluene / 24 h / Heating

With dmap; sulfuric acid; p-toluenesulfonylanhydride; water; ammonium formate; silica gel; diisobutylaluminium hydride; sodium hydrogencarbonate; triethylamine; para-thiocresol; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1021/jo000250y

Reference yield:

: 362517-07-5
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2S)-2-ethyl-2,3-dihydroxypropyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362517-19-9
C₃₃H₄₀N₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96.1 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

2.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

3.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

4.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

5.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

5.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

6.1: thiocresol / 2 h / 110 °C

6.2: 2.458 g / tributyltin hydride; 2,2'-azobisisobutyronitrile / toluene / 24 h / Heating

With dmap; p-toluenesulfonylanhydride; ammonium formate; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; para-thiocresol; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; acetone; benzene;
DOI:10.1021/jo000250y