methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

Base Information

Chemical Name:methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate
CAS No.:1430328-32-7
Molecular Formula:C₁₆H₂₁NO₄S
Molecular Weight:323.413
Hs Code.:

Synonyms:methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

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Chemical Property of methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

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Technology Process of methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

There total 5 articles about methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₁NO₂S

: 1430328-32-7
methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.12.031

Reference yield:

: 6320-01-0
3-Bromothiophenol

: 1430328-32-7
methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 2 h / Reflux

2.1: magnesium; iodine / diethyl ether / Inert atmosphere; Heating

2.2: 1 h / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 15 h / Reflux

4.1: triethylamine / dichloromethane / 2 h / 0 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C

With iodine; potassium carbonate; magnesium; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.ejmech.2012.12.031

Reference yield:

: 70398-87-7
1-bromo-3-isopropylsulfanylbenzene

: 1430328-32-7
methyl 4-(3-isopropylsulfonylphenyl)-3,6-dihydro-2H-pyridine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium; iodine / diethyl ether / Inert atmosphere; Heating

1.2: 1 h / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 15 h / Reflux

3.1: triethylamine / dichloromethane / 2 h / 0 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C

With iodine; magnesium; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1016/j.ejmech.2012.12.031