1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate

Base Information

• Chemical Name: 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate
• CAS No.: 1607442-60-3
• Molecular Formula: BF₄*C₁₁H₁₁F₃N₃O
• Molecular Weight: 345.028
• Mol file: 1607442-60-3.mol

Synonyms:1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate

Chemical Property of 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate

There total 2 articles about 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazole 1-oxide (1607442-58-9) + trimethoxonium tetrafluoroborate (420-37-1) → 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate (1607442-60-3)

Guidance literature:

In dichloromethane; at 23 ℃; for 65h;

Reference yield:

4-(trifluoromethyl)phenylhydrazine (368-90-1) → 1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate (1607442-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diethyl ether / 2 h / 23 °C

1.2: 17 h / Reflux

2.1: dichloromethane / 65 h / 23 °C

In diethyl ether; dichloromethane;

Reference yield:

1-methoxy-4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazolium tetrafluoroborate (1607442-60-3) → 4-methoxy-5-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazole (1607442-61-4)

Guidance literature:

With sodium methylate; In methanol; at 23 ℃; for 6h;

upstream raw materials:

4-(trifluoromethyl)phenylhydrazine

4-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazole 1-oxide

trimethoxonium tetrafluoroborate

Downstream raw materials:

4-methoxy-5-methyl-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazole

4-[[5-methoxy-2-[4-(trifluoromethyl)phenyl]-2H-1,2,3-triazol-4-yl]methyl]-2-(trifluoromethyl)pyridine

4-methoxy-2-[4-(trifluoromethyl)phenyl]-5-[[3-(trifluoromethyl)-1H-pyrazol-1-yl]methyl]-2H-1,2,3-triazole

4-methyl-2-[4-(trifluoromethyl)phenyl]-5-[[5-(trifluoromethyl)-3-thienyl]oxy]-2H-1,2,3-triazole